I am trying to determine the most ancient extant source for the concept of Hell as a place of spiritual cleansing. Regardless of what term you use for it (etc. ,גיא בן הינום, שְׁאוֹל), I understand that most Jews teach that Hell is a place of spiritual cleansing prior to entering the world to come (גַּן עֵדֶן "heaven," העולם הבא, etc.). What I am wondering is how far back this teaching can be substantiated. Who is the most ancient source making this claim and approximately what time period was it made? For instance, another user mentioned Nachmanides in Sha'ar HaGemul quoting Pirkei D'Rabbi Eliezer concerning שְׁאוֹל as well as some other sources, when would these have been written (approximately)? Are there any older sources?
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The belief in reward and punishment in the afterlife is a fundamental tenet of the Jewish faith (11th Principle of Rambam's 13 Principles of Faith). The earliest references I know of are various references in the Babylonian Talmud. Rosh Hashana 16b-17a attributes the view to Bais Shammai (ca 1st Century C.E.). Rabbi Akiva (ca 40 CE - ca 137 CE) is a bit more specific about how the non-wicked but less than righteous would be cleansed in Gehinnom for not more than 12 months. Mishna, Eduyos 2:10.
Although the books of the Tanach (i.e. the Hebrew Bible) allude to the afterlife, as the Talmudic citations above reveal, it is not very specific which is one reason the Sadducee sect refused to recognize the concept. See Josephus, Antiquities of the Jews, Book 18 Chapter 1. Our sages of the late Second Temple (sometimes known as the Pharisees), held to the belief in reward and punishment after death as a lesson of the Oral Torah -- the unwritten detailing of laws given by G-d to Moses and passed down generation to generation thereafter.
Pirkei deRabbi Eli'ezer is a compilation of midrashim [rabbinic allegory and exegesis], and the dating is questionable but scholars generally assign it to the eighth or ninth century. My reading of that source, though, doesn't say anything about Sheol as a place of cleansing the soul, but simply that Sheol is the lowest of the seven levels of Gehinnom.
As for your question, one of the earliest Jewish sources in my mind would be the (Babylonian) Talmud (completed circa 500 CE). The (Hebrew) Bible doesn't mention anything about She'ol as a place of cleansing — in the TaNaKh, She'ol is simply the place where a person's life-force goes when they die. In the Talmud, however, we read (Rosh haShana 16b-17a):
Later on this same page, the rabbis discuss the different kinds of people who go to Gehinnom and the lengths of time they need to spend there.
I'm far from a Talmudic scholar, so I'm sure the other knowledgeable users on this site will have additional, illuminating comments to add.